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E mild reaction circumstance, low cost, abundant workup procedure and good to first-class yields as advisable as the CRO for using broad substrates make our methodology a semiprecious contribution to the existing processes for synthesis of benzimidazole.
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Benzimidazole synthesis
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How is the recrystallisation of benzimidazole done?
Recrystallisation: Dissolve the synthesized product in 400 ml of boiling water, add 2 g of decolourising carbon and digest for 15 min. Filter rapidly through a preheated Buchner funnel and a flask at the pump. Cool the filtrate to about 10 °C, filter off the benzimidazole, wash with 25 ml of cold water and dry at 100 °C.
How to calculate benzimidazole yield from o-phenylenediamine?
Cool the filtrate to about 10 °C, filter off the benzimidazole, wash with 25 ml of cold water and dry at 100 °C. The yield of pure benzimidazole, m.p. 171-172 °C, is 25 g (85%). Here limiting reagent is o-phenylenediamine; hence yield should be calculated from its amount taken.
How is a mono acyl derivative converted to a benzimidazole?
Mono acyl derivative of o-phenylenediamine is readily converted into the corresponding benzimidazole by the action of heat alone. These conversions are generally carried out at a temperature somewhat above the melting point of the starting compounds.
Which is the best example of benzimidazole synthesis?
Synthesis of commercially available benzimidazole involves condensation of o-phenylenediamine with formic acid. The most prominent benzimidazole compound in nature is N-riosyldimethylbenzimidazole, which serves as a axial ligand for cobalt in vitamin B12.
Last Update: Oct 2021
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